Re: [ccp4bb] L-alanosine

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Subject: Re: L-alanosine
From: Ian Ollmann iano {- at -} APPLE {- dot -} COM
Date: 2007-07-05

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Date: 2007-07-05

Subject: Re: L-alanosine
From: "Das, Debanu" debanu {- at -} SLAC {- dot -} STANFORD {- dot -} EDU
Date: 2007-07-05

Hi Jackie,
It seems that when the crystal structure of L-alanosine was solved, it was done from a solution made by adding conc. HCl (20 ul) to the compound in water (200 ul).

See ref. in Acta Cryst., 1986, C42, 733-738.

I don't know what the starting pH of the compound in water will be, but I think you can try the above ratio or else try to get the pH between 8-9.

Thanks,
Debanu.

________________________________

From: CCP4 bulletin board on behalf of Jacqueline Vitali
Sent: Thu 7/5/2007 6:12 PM
To: CCP4BB@JISCMAIL.AC.UK
Subject: [ccp4bb] L-alanosine

Dear colleagues,

Does anyone know how to dissolve L-alanosine? It is not very soluble in water.

Thanks.

Jackie Vitali

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CCP4bb <-- 2007 <-- July 2007 <-- 05 July 2007

Previous message:
Subject: Re: L-alanosine
From: Ian Ollmann iano {- at -} APPLE {- dot -} COM
Date: 2007-07-05

Next message:
Subject: Re: The CCP4 license is ambiguous
From: Tim Grune tim {- dot -} grune {- at -} SYNCHROTRON {- dot -} VIC {- dot -} GOV {- dot -} AU
Date: 2007-07-05